|
Sign In to gain access to subscriptions and/or personal tools.
|
A Scanning Electron Microscopic Investigation of Bonding of Methacryloyloxyalkyl Hydrogen Maleate to Etched Dentin
T. Fukushima
Department of Dental Materials and Devices, Fukuoka Dental College, 700 Ta, Sawara-ku, Fukuoka 814-01, Japan
T. Horibe
Department of Dental Materials and Devices, Fukuoka Dental College, 700 Ta, Sawara-ku, Fukuoka 814-01, Japan
Three types of methacryloyloxyalkyl hydrogen maleates-2-(methacryloyloxy)ethyl hydrogen maleate (2MEM), 1-(methacryloyloxymethyl)ethyl hydrogen maleate (MMEM), and 1-(methacryloyloxymethyl)propyl hydrogen maleate (MMPM)-were prepared for use as bonding agents. The relationships between the thickness of an acid-proof dentin layer and the bond strength and chemical structure of the synthesized monomers were investigated. The bond strengths of 2MEM/composite system to dentin treated with either 37% phosphoric acid solution or 10% citric acid-3% ferric chloride solution (10-3 solution) were superior to those of the others. The acid-proof dentin layer for all bonding agents containing the synthesized monomers at the resin-dentin interface was clearly visible in a scanning electron microscope, regardless of the types of dentin etching agents used. After treatment of the dentin with the phosphoric acid solution, the layers of 2MEM, MMEM, and MMPM were 5-6 µm, 3-4 µm, and 2-3 µm thick, respectively. When the dentin was treated with the 10-3 solution, the layer for each bonding agent was approximately 1 µm thick.
REFERENCES
- Abe, Y. (1986): Relation between Interpenetration and Bond Strength to Dentin with 4-META, Pheny-P, HNPM, and 4-MET/MMA-TBB Resins, J Jpn Dent Mater 5:839-851.
- Asmussen, E. and Munksgaard, E.C. (1985): Adhesion of Restorative Resins to Dentinal Tissues. In: Posterior Composite Resin Dental Restorative Materials, G. Vanherle and D.C. Smith, Eds., Utrecht: Peter Szulc Publishing Co., pp. 217-229.
- Banting, D.W.; Ellen, R.P.; and Fillery, E.D. (1985): A Longitudinal Study of Root Caries: Baseline and Incidence Data, J Dent Res 64:1141-1144.[Abstract/Free Full Text]
- Beck, J.D.; Hunt, R.J.; Hand, J.S.; and Field, H.M. (1985): Prevalence of Root and Coronal Caries in a Noninstitutionalized Older Population, J Am Dent Assoc 111:964-967.[Abstract]
- Bowen, R.L. (1980): Adhesive Bonding of Various Materials to Hard Tooth Tissues. XXII. The Effects of a Cleanser, Mordant, and PolySAC on Adhesion Between a Composite Resin and Dentin, J Dent Res 59:809-814.
- Bowen, R.L. and Cobb, E.N. (1983): A Method for Bonding to Dentin and Enamel, J Am Dent Assoc 107:734-736.[Abstract]
- Bowen, R.L.; Cobb, E.N.; and Rapson, J.E. (1982): Adhesive Bonding of Various Materials to Hard Tooth Tissues: Improvement in Bond Strength to Dentin, J Dent Res 61:1070-1076.[Abstract/Free Full Text]
- Brannstrom, M. (1985): Composite Resin Restorations: Biological Considerations with Special Reference to Dentin and Pulp. In: Posterior Composite Resin Dental Restorative Materials, G. Vanherte and D.C. Smith, Eds., Utrecht: Peter Szulc Publishing Co., pp. 71-81.
- Brännström, M. and Nordenvall, K.J. (1978): Bacterial Penetration, Pulpal Reaction and the Inner Surface of Concise Enamel Bond. Composite Fillings in Etched and Unetched Cavities, J Dent Res 57:3-10.[Abstract/Free Full Text]
- Eliades, G.C.; Caputo, A.A.; and Vougiouklakis, G.J. (1985): Composition, Wetting Properties and Bond Strength with Dentin of 6 New Dentin Adhesives, Dent Mater 1:170-176.[CrossRef][Medline]
[Order article via Infotrieve]
- Fujitani, M. (1986): Effects of Acid-etching, Marginal Microleakage, and Adaptation to Dentinal Wall on the Dental Pulp in Adhesive Composite Restorations, Jpn J Conserv Dent 29:228-253.
- Fukushima, T.; Inoue, Y.; and Horibe, T. (1988): Synthesis of 2-Methacryloxyethyl Hydrogen Maleate and Its Bonding to Tooth Surfaces, J Jpn Dent Mater 7:675-679.
- Fukushima, T.; Kawaguchi, M.; Inoue, Y.; Miyazaki, K.; and Horibe, T. (1985): Application of Functional Monomers for Dental Use (Part-9) Syntheses of Succinoxy Methacrylates and Their Adhesion to Polished and Etched Tooth Surfaces, Dent Mater J 4:33-39.[Medline]
[Order article via Infotrieve]
- Herrin, H.K. and Shen, C. (1985): Microleakage of Root Caries Restorations, Gerodontics 1:156-159.[Medline]
[Order article via Infotrieve]
- Jedrychowski, J.R.; Caputo, A.A.; and Prola, J. (1981): Influence of a Ferric Chloride Mordant Solution on Resin-dentin Retention, J Dent Res 60:134-138.[Abstract/Free Full Text]
- Kadoma, Y. and Imai, Y. (1988): Effect of Ferric Salts on Polymerization of MMA-A Model to Study the Mechanism of Adhesion of MMA Resin to Dentin, J Jpn Dent Mater 7:817-823.
- Kato, H.; Wakumoto, S.; and Suzuki, M. (1986): Chemical Analysis of Interface Layer between Resin and Dentine by Raman Microprobe,.J Jpn Dent Mater 5:232-237.
- Kohyama, H. (1988): Pulpal Response of Human Dental Pulp to an Adhesive-Light-Cured Composite Resin Restoration System and Observation of Contact Area between Composite Resin and Dentin, Jpn J Conserv Dent 31:352-387.
- Miyairi, H. and Fukuda, H. (1987): A Shear Test Method of Dental Adhesives, J Jpn Dent Mater 6:614-620.
- Mizunuma, T. and Nakabayashi, N. (1986): Relationship between Bond Strength and Structure of Dentin Collagen-Adhesion to Dentin with 4-META/MMA-TBB Resin, J Jpn Dent Mater 5:471-474.
- Munksgaard, E.C. and Asmussen, E. (1984): Bond Strength Between Dentin and Restorative Resins Mediated by Mixtures of HEMA and Glutaraldehyde, J Dent Res 63:1087-1089.[Abstract/Free Full Text]
- Nakabayashi, N.; Takeyama, M.; Kojima, K.; and Ma-Suhara, E. (1982): Studies on Dental Self-Curing Resins {19)-Adhesion of 4-META/MMA-TBB Resin to Pretreated Dentine, J Jpn Soc Dent Apparatus Mater 23:29-33.
- Nakajima, A. (1985): Bond Strength of Adhesive Composite Resins, Part 2. Adhesive Property of a New Bonding Agent to Tooth Substances and Adhesion Structures in the Dentin, Jpn J Conserv Dent 28:850-865.
- Nakamichi, I.; Iwaku, M.; and Fusayama, T. (1983): Bovine Teeth as Possible Substitutes in the Adhesion Test, J Dent Res 62:1076-1081.[Abstract/Free Full Text]
- Nordenvall, K.J.; Brännström, M.; and Torstenson, B. (1979): Pulp Reactions and Microorganisms under ASPA and Concise Composite Fillings, ASDC J Dent Child 46:449-453.[Medline]
[Order article via Infotrieve]
- Retief, D.H.; Austin, J.C.; and Fatti, L.P. (1974): Pulpal Response to Phosphoric Acid, J Oral Pathol 3:114-122.[Medline]
[Order article via Infotrieve]
- Rider, M.; Tanner, A.N.; and Kenny, B. (1977): Investigation of Adhesive Properties of Dental Composite Materials Using an Improved Tensile Test Procedure and Scanning Electron Microscopy, J Dent Res 56:368-378.[Abstract/Free Full Text]
- Stanley, H.R.; Going, R.E.; and Chauncey, H.H. (1975): Human Pulp Response to Acid Pretreatment of Dentin and to Composite Restoration, J Am Dent Assoc 91:817-825.[Abstract]
- Torstenson, B.; Nordenvall, K.J.; and Brannstrom, M. (1982): Pulpal Reaction and Microorganisms under Clearfil Composite Resin in Deep Cavities with Acid Etched Dentin, Swed Dent J 6:167-176.[Medline]
[Order article via Infotrieve]
Journal of Dental Research, Vol. 69, No. 1,
46-50 (1990)
DOI: 10.1177/00220345900690010701
 CiteULike  Complore  Connotea  Del.icio.us  Digg  Reddit  Technorati  Twitter What's this?
This article has been cited by other articles:
|
|
|
|
 
J. Perdigao, E.J. Swift Jr, G.E. Denehy, J.S. Wefel, and K.J. Donly
In vitro Bond Strengths and SEM Evaluation of Dentin Bonding Systems to Different Dentin Substrates
Journal of Dental Research,
January 1, 1994;
73(1):
44 - 55.
[Abstract]
[PDF]
|
|
|
|
|
|
|
B. Van Meerbeek, S. Inokoshi, M. Braem, P. Lambrechts, and G. Vanherle
Morphological Aspects of the Resin-Dentin Interdiffusion Zone with Different Dentin Adhesive Systems
Journal of Dental Research,
August 1, 1992;
71(8):
1530 - 1540.
[Abstract]
[PDF]
|
|
|
|
|
