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Glass-ionomer Cement Formulations. II. The Synthesis of Novel Polycarboxylic Acids
Stephen Crisp
Laboratory of the Government Chemist, Cornwall House, Stamford Street, London SE1 9NQ, England
Brian E. Kent
Laboratory of the Government Chemist, Cornwall House, Stamford Street, London SE1 9NQ, England
Brian G. Lewis
Laboratory of the Government Chemist, Cornwall House, Stamford Street, London SE1 9NQ, England
Alan J. Ferner
Laboratory of the Government Chemist, Cornwall House, Stamford Street, London SE1 9NQ, England
Alan D. Wilson
Laboratory of the Government Chemist, Cornwall House, Stamford Street, London SE1 9NQ, England
The synthesis of many polycarboxylic acids is reported. An account is given of their stability in aqueous solution and the properties of cements formed by their reaction with ion-leachable glasses. A copolymer of acrylic and itaconic acids was found to combine several favorable characteristics.
REFERENCES
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- Crisp, S.; Lewis, B.G.; and Wilson, A.D.: Gelation of Polyacrylic Acid Aqueous Solutions and the Measurement of Viscosity, J Dent Res 54:1173-1175, 1975.[Abstract/Free Full Text]
- Crisp, S.; Ferner, A.J.; Lewis, B.G.; and Wilson, A.D.: Properties of Improved Glass-ionomer Cement Formulations, J Dent 3:125-130,1975.[CrossRef][Medline]
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- Williams, J.W. (Ed.): Ultracentrifugal Analysis in Theory and Experiment. New York and London: Acad. Press, 1963.
- Peaker, F.W.: Light-scattering Techniques in Techniques of Polymer Characterization. P. W. Allen (Ed.), London: Butterworths, 1959, Chap. 5.
- Crisp, S.; Lewis, B.G.; and Wilson, A.D.: Characterization of Glass-ionomer Cements. 3. Effect of Polyacid Concentration on the Physical Properties, J Dent 5:51-56, 1977.[CrossRef][Medline]
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- Wilson, A.D.; Crisp, S.; and Ferner, A.J.: Reactions in Glass-ionomer Cements. IV. Effect of Chelating Comonomers on Setting Behavior, J Dent Res 55:489-495, 1976.[Abstract/Free Full Text]
- Crisp, S. and Wilson, A.D.: Reactions in Glass-ionomer Cements. V. Effect of Incorporating Tartaric Acid in the Liquid, J Dent Res 55:1023-1031, 1976.[Abstract/Free Full Text]
- Wilson, A.D.; Crisp, S.; and Abel, G.: Characterization of Glass-ionomer Cements. 4. Effect of Molecular Weight on Physical Properties, J Dent 5:117-120, 1977.[CrossRef][Medline]
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- Muto, N.: Counterion Effect on the Titration Behavior of Poly(Maleic) Acid, Bull Chem Soc Jap 47:1122-1128, 1974.[CrossRef]
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Journal of Dental Research, Vol. 59, No. 6,
1055-1063 (1980)
DOI: 10.1177/00220345800590060801
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