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Journal of Dental Research
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Semiporous Reinforcing Fillers for Composite, Resins: II. Heat Treatments and Etching Characteristics

R.L. Bowen

American Dental Association Health Foundation, Research Unit at the National Bureau of Standards, Washington, DC 20034, USA

L.E. Reed

American Dental Association Health Foundation, Research Unit at the National Bureau of Standards, Washington, DC 20034, USA

Candidate experimental semiporous reinforcing filler particles were prepared by heat treatment of certain glass compositions, followed by crushing and etching. Optical microscopic techniques were aided by the use of certain dyes and staining procedures to manifest submicroscopic interconnected porosity in the surface of the particles. The goal of this endeavor was to develop semiporous glass reinforcing fillers for the improvement of dental composite materials.

REFERENCES

  • Bowen, R.L., and Reed, L.E.: Semiporous Reinforcing Fillers for Composite Resins: I. Preparation of Provisional Glass Formulations, J Dent Res 55: 738-747, 1976.
  • Hood, H.P., and Nordberg, M.E.: Treated Borosilicate Glass, U.S. Patent 2,106,744, 1938.
  • Gurr, E.: Synthetic Dyes in Biology, Medicine and Chemistry, New York, Academic Press Inc., 1971, p 76.
  • Bowen, R.L., and Cleek, G.W.: A New Series of X-Ray-Opaque Reinforcing Fillers for Composite Materials, J Dent Res 51: 177-182, 1972.
  • Patty, F.A. (ed): Industrial Hygiene and Toxicology, Vol II, 2nd revised ed, New York: Interscience Publishers, 1962, pp 1000, 1131.
  • Sacks, N.I.: Dangerous Properties of Industrial Materials, New York: Reinholdt Publishing Corp., 1957, p 1138.
  • Bowen, R.L.: Properties of a Silica-Reinforced Polymer for Dental Restorations, JADA 66: 57-64, 1963.
  • Elmer, T.H.; Nordberg, M.E.; Carrier, G.B.; and Korda, E.J.: Phase Separation in Borosilicate Glasses as Seen by Electron Microscopy and Scanning Electron Microscopy, J Am Ceramic Soc 53: 171-175, 1970.
  • Moriya, Y.; Warrington, D.H.; and Douglas, R.W.: A Study of Metastable Liquid-Liquid Immiscibility in Some Binary and Ternary Alkali Silicate Glasses, Phys Chem Glasses 8: 19-25, 1967.
  • Bowen, R.L.: Effect of Particle Shape and Size Distribution in a Reinforced Polymer, JADA 69:481-495, 1964.

Journal of Dental Research, Vol. 55, No. 5, 748-756 (1976)
DOI: 10.1177/00220345760550050801


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This Article
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