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Figure 1A. Liquid-state 13C NMR spectra of the collagen, before and after heat treatment. The accumulation and repetition times were 84,000 and 3.8 sec, respectively. The hexamethyl-di-siloxane was used as an external reference. The upper spectrum was obtained before heat treatment. The lower spectrum was obtained after heat treatment.
J DENT RES, Vol. 82, No. 4,
257-261 (2003)
DOI: 10.1177/154405910308200403
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