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Journal of Dental Research
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Setting and Thermal Reactions of Phosphate Investments

Robert Neiman

Whip-Mix Corporation, Inc., 361 Farmington Avenue, Louisville, Kentucky 40217

Atul C. Sarma

Whip-Mix Corporation, Inc., 361 Farmington Avenue, Louisville, Kentucky 40217

The setting reactions and thermal degradation of the phosphate binders are interpreted from the DTA and X-ray diffraction data. Setting takes place through complex formation of (NH4Mg PO4.6H2O)n, excess reactants, and water. Dehydration and thermal reactions lead to a sequence of reactions forming (NH4MgPO4.H2O) n, (Mg2P2 O7)n', Mg2P 2O7, and Mg3(PO4)2.

Journal of Dental Research, Vol. 59, No. 9, 1478-1485 (1980)
DOI: 10.1177/00220345800590090401
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